Qiu, Chunlei (2010). Net-shape hot isostatic pressing of a nickel-based powder superalloy. University of Birmingham. Ph.D.
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Qiu10PhD.pdf
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Abstract
Microstructural analysis and mechanical property assessment have been carried out on hot isostatically pressed (HIPped) and heat treated samples of RR 1000 powder to assess Net Shape HIPping as a process-route for aero engine components. HIPping led to (Hf,Zr)-rich oxides and carbides on prior particle boundaries (PPBs) which could be coarsened, but not eliminated by changing the HIP procedure. HIPping above the γ′ solvus resulted in coarser grains with serrated boundaries and in the formation of irregular-shaped secondary γ′ and fan-type γ-γ′ structures. Factors which influence the growth and morphology of γ′ particles are considered and it is shown that particle impingement dominates in the formation of irregular γ′ during continuous cooling from supersolvus. Solution treatment near the HIPping temperature led to thermally induced pores (TIP) but lower temperatures avoided TIP and changed the γ′ size, distribution and morphology giving a large volume fraction of finer cuboidal secondary γ′ and medium-sized spherical tertiary γ′.
Type of Work: | Thesis (Doctorates > Ph.D.) | |||||||||
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Award Type: | Doctorates > Ph.D. | |||||||||
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College/Faculty: | Colleges (2008 onwards) > College of Engineering & Physical Sciences | |||||||||
School or Department: | School of Metallurgy and Materials | |||||||||
Funders: | Other | |||||||||
Other Funders: | Overseas Research Students Awards Scheme, The University of Birmingham | |||||||||
Subjects: | T Technology > T Technology (General) T Technology > TN Mining engineering. Metallurgy |
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URI: | http://etheses.bham.ac.uk/id/eprint/1255 |
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