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http://eprints.org/relation/isVolatileVersionOf http://etheses.bham.ac.uk/id/document/1425 http://eprints.org/relation/ispreviewThumbnailVersionOf http://etheses.bham.ac.uk/id/document/1425 http://eprints.org/relation/isVersionOf http://etheses.bham.ac.uk/id/document/1425 archive 4031 disk0/00/00/05/92 2010-03-26 12:07:40 2019-01-23 09:52:27 2011-07-19 16:20:00 thesis show 0 Lee Tae Jung Kendall Kevin University of Birmingham unpub TP QD 10col_ephy The optimisations of reduction and operation of Ni-YSZ anode supported micro tubular cells on pure methane were studied. A major problem of SOFCs is nickel anode performance on methane and higher hydrocarbons. The aim of this work was to study the effect of reduction and operation of anode-supported microtubular SOFCs using methane as both reductant and fuel. The results were compared to those from optimised operation using hydrogen. To measure mechanical strength, the three point bending test was employed. Temperature programmed oxidation (TPO) results were investigated to measure the carbon deposition on the anode in order to assess potential damage to the cermet catalyst. Also field emission scanning electron microscope (FE-SEM) and Energy-Dispersive X-ray spectroscopy EDS results were analysed on the anode surface. 2010-07 2009 graduation eng author unchecked This unpublished thesis/dissertation is copyright of the author and/or third parties. The intellectual property rights of the author or third parties in respect of this work are as defined by The Copyright Designs and Patents Act 1988 or as modified by any successor legislation. Any use made of information contained in this thesis/dissertation must be in accordance with that legislation and must be properly acknowledged. Further distribution or reproduction in any format is prohibited without the permission of the copyright holder. public 148 University of Birmingham School of Chemical Engineering d_ph FALSE na 2010-07 graduation