Mesopore immobilised bis(oxazoline) catalysts for enantioselective catalysis

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http://eprints.org/relation/isVersionOf http://etheses.bham.ac.uk/id/document/21664 http://eprints.org/relation/isVolatileVersionOf http://etheses.bham.ac.uk/id/document/21664 http://eprints.org/relation/isIndexCodesVersionOf http://etheses.bham.ac.uk/id/document/21664 archive 4031 disk0/00/00/35/78 2012-07-13 11:13:06 2019-01-23 09:56:36 2012-07-13 11:13:06 thesis show 0 Clarke Richard John Shannon Ian University of Birmingham Mesopore immobilised bis(oxazoline) catalysts for enantioselective catalysis unpub QD 30sch_chem Mesoporous silica materials have the potential to replace many conventional silicas for uses such as supports for heterogeneous catalysis and absorbents. The large pore size and high surface area make them ideal for supporting bulky organometallic catalysts for enantioselective reactions. We have immobilised chiral bis(oxazoline) metal complexes onto the surfaces of some of these versatile supports (MCM-41 and MCM-48) via different tethering strategies. The resulting heterogeneous catalysts were shown to be highly active in the enantioselective cyclopropanation of styrene with ethyl diazoacetate. 2003-07-21 2003-01 graduation 2262205 eng other Scanned by Hollingworth and Moss This unpublished thesis/dissertation is copyright of the author and/or third parties. The intellectual property rights of the author or third parties in respect of this work are as defined by The Copyright Designs and Patents Act 1988 or as modified by any successor legislation. Any use made of information contained in this thesis/dissertation must be in accordance with that legislation and must be properly acknowledged. Further distribution or reproduction in any format is prohibited without the permission of the copyright holder. public 250 University of Birmingham School of Chemistry d_ph na 2003-07-21 graduation